Short-Path Distillation System

Short-Path Distillation System

Model: RSP-SD

The proposed FLOSN RSP-SD is a laboratory wiped-film short-path platform for feasibility studies on compatible low-volatility or thermally sensitive mixtures. Metered feed forms a thin film on the heated wall, while a central condenser collects vapor over a short travel distance. Separate distillate and residue receivers support mass-balance evaluation. The baseline is a small continuous-feed trial system with finite collection capacity, not an unlimited continuous-production plant.

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FLOSN / PRODUCT FEATURES

Product Features

6 FEATURES

True Internal Condenser Layout

Keeps the main condensing surface inside the evaporator rather than using an external condenser as the defining element.

Controlled Film Formation

Variable wiper speed and metered feeding support trials on film coverage and fouling.

Independent Thermal Circuits

Separately sets evaporator-wall and internal-condenser conditions.

Separated Product Streams

Distinct collection paths support distillate/residue yield and composition measurements.

Visible Process Development

Guarded glass construction permits observation of film distribution, foam and deposition.

Vapor-Load-Aware Vacuum

Cold trapping, line conductance and feed rate are assessed together.

FLOSN / TECHNICAL PARAMETERS

Product Features

SELECTED MODEL

CFD-SA1000

Model-specific specifications
Chamber volume
1,080 mL
Operating pressure
0–2,200 psi
Power consumption
1,500 W
Exhaust flow rate
0–2 SLPM

Chamber & operation

Chamber dimensions · I.D. × depth (mm)
165.1 × 50.8 mm
Chamber dimensions · I.D. × depth (in)
6.5 × 2 in
Operating pressure · MPa
0–15.2 MPa
Maximum safe working pressure
2,500 psi (17.2 MPa)
Heating method
Cartridge heater heating
Overall dimensions · W × D × H
Not specified
SELECTED MODEL

CFD-SA1800

Model-specific specifications
Chamber volume
1,860 mL
Operating pressure
0–2,200 psi
Power consumption
2,000 W
Exhaust flow rate
0–0.5 SLPM

Chamber & operation

Chamber dimensions · I.D. × depth (mm)
215.9 × 50.8 mm
Chamber dimensions · I.D. × depth (in)
8.5 × 2 in
Operating pressure · MPa
0–15.2 MPa
Maximum safe working pressure
2,500 psi (17.2 MPa)
Heating method
Cartridge heater heating
Overall dimensions · W × D × H
Not specified
Shared specifications · all models

Materials & pressure safety

Chamber material
SS316L
Optional materials
Hastelloy C276, Inconel 625, Monel 400, Titanium Grade 2, PTFE lining
Pressure safety system
Electronic pressure monitoring combined with mechanical over-pressure relief protection

Environment & utilities

Operating temperature range
−30 to +60 °C
Operating ambient humidity
20%–70% RH, non-condensing
Power supply
120 / 220 V AC, 50–60 Hz
CO₂ gas requirement
High-purity liquid CO₂ supply; recommended purity >99.9%

Cooling, control & filtration

Cooling system
Integrated closed-loop cooling; the internal chiller loop accelerates cooling and reduces CO₂ consumption
Control system
LCD touchscreen; semi-automated control with programmable timer operation and electronic sensor monitoring
Filtration system
Double T-Filter, Cat. No. 8785; two passes through 0.5 μm filters; >99.5% retention

Samples & chemical compatibility

Compatible sample types
Biological specimens, microscopy samples, hydrogels, aerogels, porous materials, polymers, and other structure-sensitive materials
Compatible solvents
CO₂-miscible solvents commonly used in sample preparation, including ethanol, acetone, methanol, and other laboratory solvents
Chemical compatibility warning
Strongly acidic, strongly alkaline, oxidizing, or highly toxic solvents require prior compatibility evaluation before use
Standard configuration & options

Standard configuration

  • High-pressure viewing window chamber
  • Integrated chamber illumination system
  • Integrated condensation and gas-liquid separation system
  • Non-mechanical CO₂ mixing and exchange system
  • Controlled slow filling and venting system
  • Precision vent flow meter
  • Standard stainless steel CO₂ supply line
  • Anti-static exhaust tubing
  • Replacement O-ring seal kit
  • Installation tool kit
  • User operation manual
  • Factory acceptance test report
  • Warranty and technical support

Optional configurations

  • Interchangeable sample holders
  • Custom sample chamber inserts
  • Magnetic stirring module
  • High-temperature / high-pressure chamber customization
  • Corrosion-resistant alloy chamber upgrade
  • Microscopy sample holder kit

FLOSN / APPLICATIONS

Applications

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